SiLi Spectrometer with Peltier Cooling SOL-XE/M

Application

X–ray Spectrometer based on Si(Li) detector with Peltier Cooling, model Sol-XEM is intended for conversion of X-ray photon energy into electrical signals, its amplification and analog filtration. It provides detection, accumulation and processing of X-ray spectra in situations when detector cooling by liquid nitrogen is inconvenient or impossible. It can be used for X-Ray fluorescence analysis and in X-Ray difractometry applications.

Features

  • Thermoelectric cooling of detector and input stage of preamplifier
  • Thin Be window
  • Detection of radiation in any spatial orientation
  • Closed-loop system of air cooling of Peltier cooler hot seal which provides better cooling efficiency

COMPLETE SET

Detection unit (DU) based on Si(Li) detector with thermos-electrical cooling (TC),  comprising:
  • Si(Li) detector
  • Peltier cooler
  • Vacuum chamber
  • Charge-sensitive preamplifier
  • Non Evaporable getter ( NEG ) inside vacuum chamber to support vacuum and improve peak/background 
Spectrometric device with RS-232 interface to PC, comprising:
  • Shaping processor
  • Microprocessor device with LCD display for control and diagnostic of spectrometer parameters
  • Power supply unit for TC and detector bias
  • Power supply for preamplifier
Self-contained unit for air cooling of Peltier cooler hot seal Spectrometer emulation software on CD Related cables and connectors Documentation set

DESCRIPTION

X–ray Spectrometer based on Si(Li) detector with Peltier Cooling, model Sol-XEM is intended for conversion of X-ray photon energy into electrical signals, its amplification and analog filtration.

Spectrometer provides following functions:

Accumulation and processing of X-ray spectra and spectra visualization on PC display. It gives possibility to

  • perform quantitative analysis of concentration of elements in the sample  using XRF methods
  • make calibration of diffractometric scale in several minutes
  • Establish “window” in which information is collected for establishment of diffractometric spectra, cut of background pulses and Ka spectral line from Kb spectral line of given elements. Number of outputs at least 5. The window in which may be mounted on any place in the spectrum with width 1….. 8000. 1 output can be adjusted to obtain a linear dependence of the counting rate in the window equal to the input count rate up to 200000 pulse/sec.

From WinCRM output measure intensity of spectral lines with background deduction with width of < 300 eV; it provides possibility to work without graphite monochromator and therefore increase count rates in dozens time. This option also leads to possibility to decrease X-ray tube power that is sufficient for powder samples.

The software for spectrometer emulation allows:

  • to execute spectra acquisition for the set time
  • to mark and select  regions of interest and examine them on a separate plane, increasing or reducing scale on horizontal and vertical
  • to execute energy calibration of spectra on two known energies
  • to determine centroids and area of peaks with background deduction and without background deduction
  • to carry out an automatic serial spectra acquisition with automatic record on a disk
  • to select regions of interest
  • to move a marker on a spectrum or interesting areas
  • to make an estimation of energy resolution at one second and one tenth height of full absorption peak
  • to print out spectrum window

SPECIFICATION

ParameterValue
Two shaping time constants, selectable, us2; 6
Input count rate for calibration at 6 us shaping time , cps10·103
OutputsHV
CRM
Linear Out 0-5V
Corrected WinCRM
WinCRM
RS-232
Time instability during 8 hours of continuous work, %< 0.02
Number of channels in ADC (MCA)1024; 2048; 4096; 8192
Integral non-linearity, %< 0.04
Detector bias power supply, V0-1000
LCD displayControl, diagnostics and displaying information about spectrometer conditions

SPECIFICATION

ParametersValue
Measuring X-ray radiation energies range, keV1-60
Energy resolution*, eV,
for energy 5,9 keV
for energy 59,6 keV
*at =6 s and input count rate 1 000 cps

< 195
<465
Peak to Background ratio2000:1
Nonstability of conversion coefficient for energy 26.4 keV, %< 0.06
Detector Be input windows thickness, um
Si(Li) detector sensitive surface area, mm2
Si(Li) detector thickness, mm
50
15x4
3.5
Conversion coefficient instability in operation temperature range (from +10 to +35)0С, at relative humidity up to 95% non-condensing , %/0 C< 0.02
Operating mode setting time, min< 60
Operation modeContinuous
Consumed power from alternative current with frequency (50+/-5) Hz and voltage (230+/-10%) V, W< 80
DU overall dimensions, mm200x80x98
PSM with air cooling system overall dimensions, mm355x475x175
Connective cables between DU and spectrometric device,
length, m
Network (RS232) cable length, m

4
10

FILES TO DOWNLOAD

PDF brochure

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